Halcinonide_LCMS_16357_MedChemExpress

Data File D:\\AGLIENT 1260\\DATA\\20150529\\20150529 2015-05-29 09-24-57\\BIZ2015-529-DJL9.DSample Name: BIZ2015-529-DJL9=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 37Acq. Instrument : HY-LCMS-02 Location : P1-D-03Injection Date : 5/29/2015 2:41:45 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150529\\20150529 2015-05-29 09-24-57\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 5/29/2015 9:24:57 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\WASH-COL2-5MIN.MLast changed : 5/29/2015 3:18:23 PM by Li Shan(LCMS-02) (modified after loading)Catalog No : HY-B0877 Batch#16357 A-RP-132 Additional Info : Peak(s) manually integrated DAD1 C, Sig=254,4 Ref=off (D:\\AGLIENT...60\\DATA\\20150529\\20150529 2015-05-29 09-24-57\\BIZ2015-529-DJL9.D) 2.234 1.920 2.155 2.441mAU60050040030020010000.511.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.920 MM 0.0554 3.80697 1.14588 0.1384 2 2.155 MF 0.0624 8.63493 2.30815 0.3140 3 2.234 FM 0.0613 2734.67334 743.59497 99.4364 4 2.441 MM 0.0614 3.05770 8.29390e-1 0.1112 Totals : 2750.17295 747.87839 ===================================================================== *** End of Report ***HY-LCMS-02 5/29/2015 3:18:25 PM Li Shan(LCMS-02)Page 1 of 1

Data File D:\\AGLIENT 1260\\DATA\\20150529\\20150529 2015-05-29 09-24-57\\BIZ2015-529-DJL9.DSample Name: BIZ2015-529-DJL9=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 37Acq. Instrument : HY-LCMS-02 Location : P1-D-03Injection Date : 5/29/2015 2:41:45 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150529\\20150529 2015-05-29 09-24-57\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 5/29/2015 9:24:57 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\WASH-COL2-5MIN.MLast changed : 5/29/2015 3:19:42 PM by Li Shan(LCMS-02) (modified after loading)Catalog No : HY-B0877 Batch#16357 A-RP-132 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150529\\20150529 2015-05-29 09-24-57\\BIZ2015-529-DJL9.D) ES-API, Pos, Sca 2.231350000300000250000200000150000100000500000.511.522.53min HY-LCMS-02 5/29/2015 3:19:43 PM Li Shan(LCMS-02)Page 1 of 2

Data File D:\\AGLIENT 1260\\DATA\\20150529\\20150529 2015-05-29 09-24-57\\BIZ2015-529-DJL9.DSample Name: BIZ2015-529-DJL9MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 2.231 2243575 496.20 I 457.20 I 456.20 I 455.20 I*MSD1 SPC, time=2.200:2.272 of D:\\AGLIENT 1260\\DATA\\20150529\\20150529 2015-05-29 09-24-57\\BIZ2015-529-DJL9.D ES-API,100806040 455.2Max: 135400 457.2 124.1 208.1 458.2 496.2200100200300400500600700800900m/z *** End of Report ***HY-LCMS-02 5/29/2015 3:19:43 PM Li Shan(LCMS-02)Page 2 of 2